| ID | 16337 |
| Eprint ID | 16337
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| フルテキストURL | |
| タイトル（別表記） | Urinary metabolites of organic solvents Report 1: Quantitative determination on urinary metabolites of toluene, xylene and styrene by thin-layer chromatography.
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| 著者 |
田口 豊郁
岡山大学医学部公衆衛生学教室
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| 抄録 | A simple and specific method for the quantitative determination of hippuric acid and methylhippuric acids is described. Urine samples were applied to silica gel plates (silica gel, 60 F254), and developed with chloroform- toluene-methanol-acetic acid (8:2:2:1). The spots of hippuric acid, m- or p-methylhippuric acids, o- methylhippuric acid, mandelic acid and phenylglyoxylic acid were identified by illuminating the silica gel plates with an ultraviolet lamp. The spots of hippuric acid, m- or p-methylhippuric acids and o-methylhippuric acid were scratched off and extracted with pyridine. The color was then developed with acetic anhydride and p-dimethylaminobezaldehyde (DAB) in pyridine at 40℃ for 60min. The absorbance at 458 nm was determined against a blank containing pyridine acetic anhydride and DAB.
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| キーワード | 薄層クロマトグラフィー (Thin-layer chromatography)
トルエン (Toluene)
キシレン (Xylene)
スチレン (Styrene)
生物学的暴露指標 (Biological monitoring)
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| 発行日 | 1983-08-31
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| 出版物タイトル |
岡山医学会雑誌
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| 出版物タイトル（別表記） | Journal of Okayama Medical Association
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| 巻 | 95巻
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| 号 | 7-8号
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| 出版者 | 岡山医学会
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| 出版者（別表記） | Okayama Medical Association
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| 開始ページ | 637
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| 終了ページ | 642
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| ISSN | 0030-1558
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| NCID | AN00032489
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| 資料タイプ |
学術雑誌論文
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| オフィシャル URL | https://www.jstage.jst.go.jp/article/joma1947/95/7-8/95_7-8_637/_article/-char/ja/
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| 関連URL | http://www.okayama-u.ac.jp/user/oma/index.html
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| 言語 |
日本語
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| 著作権者 | 岡山医学会
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| 論文のバージョン | publisher
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| 査読 |
有り
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| Eprints Journal Name | joma
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